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Determination of biomass burning tracers in air samples by GC/MS

Janoszka, Katarzyna Juda-Rezler, K. ; Sówka, I. ; Czaplicka, M. ; Czechowski, O. ; Majewski, G. ; Rogula-Kozłowska, W. ; Fudała, J. ; Kyzioł-Komosińska, J. ; Jabłońska-Czapla, M.

E3S Web of Conferences, 2018, Vol.28, p.1015 [Periódico revisado por pares]

Les Ulis: EDP Sciences

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Título:
Determination of biomass burning tracers in air samples by GC/MS
Autor: Janoszka, Katarzyna
Juda-Rezler, K. ; Sówka, I. ; Czaplicka, M. ; Czechowski, O. ; Majewski, G. ; Rogula-Kozłowska, W. ; Fudała, J. ; Kyzioł-Komosińska, J. ; Jabłońska-Czapla, M.
Assuntos: Air monitoring ; Air pollution ; Biomass ; Biomass burning ; Burning ; Cellulose ; Chromatography ; Environmental monitoring ; Gas chromatography ; Hydrogen bonds ; Levoglucosan ; Liquid chromatography ; Mass spectrometry ; Mass spectroscopy ; Particulate matter ; Particulates ; Pollution monitoring ; Pyridines ; Scientific imaging ; Spectroscopy ; Tracers ; Water analysis ; Water pollution ; Water sampling
É parte de: E3S Web of Conferences, 2018, Vol.28, p.1015
Descrição: Levoglucosan (LG) as a main cellulose burning product at 300°C is a biomass burning tracer. LG characterize by relatively high molar mass and it is sorbed by particulate matter. In the study of air pollution monitoring LG is mainly analyzed in particulate matter, PM 1 and PM 2,5 . The tracer create relatively high O-H…O bond and weaker C-H…O bond. Due to the hydrogen bond, LG dissolves very well in water. Analytical procedure of LG determination include: extraction, derivatization and analysis by gas chromatography coupled with mass spectrometry detector. In water samples levoglucosan is determined by liquid chromatography. The paper presents a methodology for particulate matter samples determination their analysis by gas chromatography coupled with a mass spectrometry detector. Determination of LG content in particulate matter was performed according to an analytical method based on simultaneous pyridine extraction and derivatization using N,O-bis (trimethylsilyl) trifluoroacetamide and trimethylchlorosilane mixture (BSTFA: TMCS, 99: 1).
Editor: Les Ulis: EDP Sciences
Idioma: Inglês

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Determination of biomass burning tracers in air samples by GC/MS

Janoszka, Katarzyna Juda-Rezler, K. ; Sówka, I. ; Czaplicka, M. ; Czechowski, O. ; Majewski, G. ; Rogula-Kozłowska, W. ; Fudała, J. ; Kyzioł-Komosińska, J. ; Jabłońska-Czapla, M.

Les Ulis: EDP Sciences

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