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Cation and anion electrochemically assisted solid-state transformations of malachite green

Doménech-Carbó, Antonio ; Dias, Daiane ; Domenech Carbo, Mª Teresa

The Royal Society of Chemistry 2020-01

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  • Título:
    Cation and anion electrochemically assisted solid-state transformations of malachite green
  • Autor: Doménech-Carbó, Antonio ; Dias, Daiane ; Domenech Carbo, Mª Teresa
  • Assuntos: PINTURA
  • Notas: 10.1016/S0022-0728(84)80230-2
    10.1007/s10008-013-2061-z
    10.1039/c0an00082e
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    info:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/CTQ2017-85317-C2-1-P/ES/APLICACION DE TECNICAS AVANZADAS DE MICROSCOPIA EN EL ESTUDIO DEL PATRIMONIO CERAMICO Y VITREO/
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    10.1039/b803582b
    10.1016/S0022-0728(84)80231-4
    10.1351/PAC-REP-11-11-13
    Physical Chemistry Chemical Physics
    10.1016/S0022-0728(00)00527-1
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  • Descrição: [EN] The possibility of the electrochemical promotion of different solid-to-solid transformations including the performance of successive cation and anion insertion processes has been tested using malachite green, a triphenylmethane dye, in contact with aqueous NaCl electrolyte. Electrochemical data using the voltammetry of microparticles methodology reveal significant differences with the solution phase electrochemistry of the dye. Voltammetric data, combined with atomic force microscopy, focusing ion beam-field emission scanning electron microscopy, and high-resolution field emission scanning electron microscopy permit characterization of the oxidative dissolution, oxidation with anion insertion, reduction with cation insertion and reduction with anion issue processes, whose thermochemical aspects, involving separate ion and electron transport contributions, are discussed. Financial support from the Project CTQ2017-85317-C2-1-P (Ministerio de Economia, Industria y Competitividad (MINECO), Fondo Europeo de Desarrollo Regional (ERDF) and Agencia Estatal de Investigacion (AEI)), is gratefully acknowledged. Doménech-Carbó, A.; Dias, D.; Domenech Carbo, MT. (2020). Cation and anion electrochemically assisted solid-state transformations of malachite green. Physical Chemistry Chemical Physics. 22(3):1502-1510. https://doi.org/10.1039/c9cp05835d
  • Editor: The Royal Society of Chemistry
  • Data de criação/publicação: 2020-01
  • Idioma: Inglês
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