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Method for Activation and Recycling of Trityl Resins

Redwan, Itedale Namro ; Grøtli, Morten

Journal of organic chemistry, 2012-08, Vol.77 (16), p.7071-7075 [Periódico revisado por pares]

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Título:
Method for Activation and Recycling of Trityl Resins
Autor: Redwan, Itedale Namro ; Grøtli, Morten
Assuntos: 1979 ; 1983 ; 1994 ; acid ; adwick dj ; alcohols ; Alcohols - chemistry ; Aniline Compounds - chemistry ; audhary sk ; Borates - chemistry ; Chemical Sciences ; Chemistry ; chloride ; derivatives ; en cx ; Equipment Reuse ; Exact sciences and technology ; journal of the american chemical society ; journal of the chemical society-perkin transactions 1 ; Kemi ; mild ; Noncondensed benzenic compounds ; Organic chemistry ; organic-synthesis ; p2661 ; p93 ; p95 ; peptide-synthesis ; Polystyrenes - chemistry ; Preparations and properties ; protection ; solid-phase synthesis ; tetrahedron letters ; Trityl Compounds - chemistry ; v116
É parte de: Journal of organic chemistry, 2012-08, Vol.77 (16), p.7071-7075
Notas: ObjectType-Article-1
SourceType-Scholarly Journals-1
ObjectType-Feature-2
content type line 23
Descrição: This note describes a rapid and mild strategy for the loading of alcohols and anilines onto a polystyrene triphenylmethyl (trityl) resin. High loadings were obtained in a matter of minutes by treating resin-bound trityl chloride with triethyloxonium tetrafluoroborate followed by alcohols or anilines. Yields were comparable or better than known literature methods. Recycling of the recovered resin was also possible using the developed method.
Editor: Washington, DC: American Chemical Society
Idioma: Inglês

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