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Coninuous enzymatic lubricant production from fusel oil in a two-stage packed bed reactor incorporating a water extraction column

Renata de Nazaré Vilas Bôas Rosemar de Lima; Pedro Carlos de Oliveira; Heizir Ferreira de Castro

XXII Simpósio Nacional de Bioprocessos e XIII Simpósio de Hidrólise Enzimática de Biomassas p.1-1, 2019

2019

Acesso online

  • Título:
    Coninuous enzymatic lubricant production from fusel oil in a two-stage packed bed reactor incorporating a water extraction column
  • Autor: Renata de Nazaré Vilas Bôas
  • Rosemar de Lima; Pedro Carlos de Oliveira; Heizir Ferreira de Castro
  • Assuntos: LIPASE; ENGENHARIA QUÍMICA
  • É parte de: XXII Simpósio Nacional de Bioprocessos e XIII Simpósio de Hidrólise Enzimática de Biomassas p.1-1, 2019
  • Notas: Disponível em: https://www.researchgate.net/publication/334899496_Continuous_enzymatic_lubricant_production_from_fusel_oil_in_a_two-stage_packed_bed_reactor_incorporating_a_water_extraction_column/link/5d47524fa6fdcc370a7c4baf/download?_tp=eyJjb250ZXh0Ijp7InBhZ2UiOiJwdWJsaWNhdGlvbiIsInByZXZpb3VzUGFnZSI6bnVsbH19. Acesso em: 26 fev. 2024
  • Descrição: The esterification of fusel oil with oleic acid catalyzed by lipase from Rhizopus oryzae immobilized on polystyrene/divinylbenzene copolymer resin was assessed in a two-stage packed bed reactor running on a continuous flow. Molecular sieves were used to remove the water formed as byproduct by coupling the reactor with a column extractor. The modification presented herein introduces a pathway for replacing saturated molecular sieves by regenerated sieves at a given time. Ester synthesis on a continuous flow carried out without a water column extractor was used as a control. The performance of the proposed system was quantitatively confirmed for space-times of 10 h, thus resulting in average productivities of 292.2 ± 18.5 molester g-1 min-1, with minimal feedstock lost and good stability of the immobilized lipase, revealing an average half-life time of 179.6 h.
  • Data de criação/publicação: 2019
  • Formato: p. 1-1.
  • Idioma: Inglês

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